1-(2-Hydroxyethyl)imidazolidine-2-thione (1) was obtained as a product from an in situ us polo assn mens sweaters reaction between N-(2-hydroxyethyl)ethylenediamine, carbon disulfide, potassium hydroxide, and di(4-fluorobenzyl)tin dichloride.Compound 1 was characterized by IR, UV, 1H, 13C{1H}, and 2D (COSY, NOESY, HSQC, and HMBC) NMR spectroscopies.The cyclic molecular structure was confirmed by single crystal X-ray crystallography which showed the five-membered ring to be non-planar and the π-electron density to be harry potter magsafe case localized over the CN2S chromophore.
In the crystal, thioamide⁻N⁻H…O(hydroxy) and hydroxy⁻O⁻H…S(thione) hydrogen bonds lead to supramolecular layers in the bc-plane.